VIGREUX COLUMN WITH VACUUM JACKET

Complete Micro-distillation unit consisting of a Vigreux column with vacuum jacket (effective length 150 mm) and attached Liebig condenser (jacket length approx. 160 mm), stopper with vacuum attachment, 2 x NS 14.5 cone and 1 x NS 14.5 socket joint connections, permanently fixed, plastic (PP) tubing connectors, 100 ml evaporating flask, condensate distributor with 4 x 10 ml receiving flasks, 0 to +250 °C thermometer, heating bath trough with thick Duran walls and flat-ground and polished base (capacity approx. 600 ml), stand and mountings, magnetic hotplate / stirrer, Pt1000 sensor (to control the bath temperature).

Individual components:

• Vigreux column with vacuum jacket, effective length 150 mm, attached Liebig condenser (jacket length approx. 160 mm), stopper with vacuum attachment, 2 x NS 14.5 cone and 1 x NS 14.5 socket joint connections and permanently fixed plastic (PP) tubing connectors
• Evaporating flask, 100 ml, NS 14.5 socket
• Condensate distributor,with NS 14.5 socket, 4 x NS 14.5 cones
• Receiving flask, 10 ml, NS 14.5 socket
• Set of joint clips
• Heating bath trough, glass, volume approx. 600 ml, with polished base to improve heat conduction, thick walls, compatible with magnetic hotplate / stirrer.
• Ground joint (NS 14.5) thermometer, range 0 to +250 °C, 75 mm immersion
• Stand and mountings
• Magnetic hotplate / stirrer and Pt1000 sensor (for heating bath trough)